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Chemical Components in FRUCTUS GARDENIAE

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【作者】 Tao HUANGShuzhen MUXiaojiang HAOJianxin ZHANG

【Author】 Tao HUANG;Shuzhen MU;Xiaojiang HAO;Jianxin ZHANG;Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences;

【机构】 Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences

【摘要】 [Objective]To research the chemical components in FRUCTUS GARDENIAE. [Methods]Silica column chromatography over silica gel,RP-18 reverse phase silica gel and Sephadex LH-20,as well as recrystallization were adopted. Structures of compounds were identified by1H-NMR,13C-NMR,ESI-MS,EI-MS and comparison with the data of literatures. [Results]A total of seven chemical compounds were isolated and purified from the ethanol extracts of FRUCTUS GARDENIAE,which were geniposide( 1),6α-hydroxygeniposide( 2),genipingentiobioside( 3),adian-5-en-3α-ol( 4),( 23Ζ)-cycloart-23-en-3β,25-diol( 5),7α-hydroxy sitosterol( 6) and 5,8-epidioxystigmasta-6,22-dien-3-ol( 7). [Conclusions] Compounds 4,5,6 and 7 were isolated from FRUCTUS GARDENIAE for the first time.

【基金】 Supported by the 2011 West Light Foundation of the Chinese Academy of Sciences
【所属期刊栏目】 Chemical Composition of Natural Medicine (2015年Z4期)
  • 【分类号】R284
  • 【下载频次】14
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