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On the HPLC Fingerprint of Zhuang Medicine Spilanthes paniculata Wall. ex DC.

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【作者】 Li LIFengfeng XIEPinghua YANXiangyan ZENGYi CAI

【Author】 Li LI;Fengfeng XIE;Pinghua YAN;Xiangyan ZENG;Yi CAI;Guangxi University of Chinese Medicine;

【通讯作者】 Yi CAI;

【机构】 Guangxi University of Chinese Medicine

【摘要】 [Objectives] To establish the HPLC fingerprint of Spilanthes paniculata Wall. ex DC. and provide reference for the quality control of medicinal materials. [Methods]Welch Ultimate XB-C18( 5 μm,250 mm ×4. 6 mm) chromatographic column was adopted,and the mobile phase was acetonitrile-0. 1% phosphoric acid aqueous solution for gradient elution,the detection wavelength was 328 nm,the column temperature was 25 ℃,the similarities of 18 different batches of medicinal materials were evaluated,and the HPLC fingerprint chromatogram of S. paniculata Wall. ex DC. was set up. [Results] The RSDs of precision,repeatability and stability of HPLC fingerprint of 18 batches of S. paniculata Wall. ex DC. medicine materials were all less than 3%; HPLC reference fingerprint of the medicine materials was established.[Conclusions]HPLC fingerprint was established,its data were stable and reliable,and the method was simple and efficient,which could provide reference for the quality evaluation of Zhuang medicine S. paniculata Wall. ex DC.

【基金】 Supported by"Collaborative Innovation Center in Guangxi in 2011-Study on Fingerprint of Three Kinds of Zhuang Medicine:Gynura crepidioides Benth.,Spilanthes paniculata Wall. ex DC.;Lindernia ruellioides(Colsm)Pennell.,Program of Guangxi Scientific Research and Technology Development(Gui Ke Chong 1598005-10);Zhuang Yao Medicine Collaborative Innovation Center(No.20,Gui Jiao Ke Yan[2013]);Guangxi Zhuang Yao Medicine Key Laboratory(No.32,Gui Ke Ji Zi[2014]);Guangxi Zhuang Pharmacy Key Discipline(No.16,Gui Jiao Ke Yan[2013]);Research on the Innovation Theory and Pharmacodynamics of Traditional Chinese Medicine by Guangxi Bagui Scholars(J13162)
【所属期刊栏目】 Chemical Composition of Natural Medicine (2019年03期)
  • 【DOI】10.19600/j.cnki.issn2152-3924.2019.03.005
  • 【分类号】R29
  • 【下载频次】6
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