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Study on the Quality Standard of Shema Mixture

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【作者】 Lilong YANGMin HUANG

【Author】 Lilong YANG;Min HUANG;The First Affiliated Hospital of Guangxi University of Chinese Medicine;Guangxi Zhuang and Yao Medicine Engineering Technology Research Center;

【通讯作者】 Min HUANG;

【机构】 The First Affiliated Hospital of Guangxi University of Chinese MedicineGuangxi Zhuang and Yao Medicine Engineering Technology Research Center

【摘要】 [Objectives] To establish the quality standard of Shema mixture. [Methods] Thin-Layer Chromatography(TLC) was used to qualitatively identify Ephedra sinica Stapf, Belamcanda chinensis(L.) Redouté and Citrus maxima(Burm.) Merr. cv. Tomentosa in the mixture, and High Performance Liquid Chromatography(HPLC) was established for the determination of the content of ephedrine hydrochloride, which was an effective component of principle drug E. sinica Stapf in the mixture. [Results] TLC was used to identify E. sinica Stapf, B. chinensis(L.) Redouté and C. maxima(Burm.) Merr. cv. Tomentosa in Shema mixture, and the characteristic spots were stable and clear. Ephedrine hydrochloride had a good linear relationship in the range of 2.01-14.06 μg, the average recovery of samples was 98.77%, RSD=1.58%. [Conclusions] TLC and HPLC, as the quality control methods of Shema mixture, have high accuracy and good repeatability, which laid a foundation for the quality control of Shema mixture.

【基金】 Supported by Open Project of Guangxi Zhuang and Yao Medicine Engineering Technology Research Center,No.KJT4190010
【所属期刊栏目】 Processing of Traditional Chinese Medicine and Quality Control (2020年03期)
  • 【DOI】10.19600/j.cnki.issn2152-3924.2020.03.011
  • 【分类号】O657.7;TQ460.72
  • 【下载频次】1
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