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Synthesis,Crystal Structure and Properties of a Zinc(Ⅱ) Complex Based on 5-(1H-Tetrazol-5-yl)isophthalic Acid Ligand

张兴晶王璐瑶尉兵李梦乔宇车广波

  College of Chemistry,Jilin Normal University    Key Laboratory of Preparation and Applications of Environmental Friendly Materials,Chinese Ministry of Education,Jilin Normal University  

摘要:A novel polymeric zinc(II) complex {[Zn2(TIA)(H2O)3]?(NO3)}n(1, H3TIA = 5-(1H-tetrazol-5-yl)isophthalic acid) has been synthesized in mixed solvents under solvothermal conditions and characterized by elemental analysis, IR spectroscopy and X-ray single-crystal diffraction. Complex 1 crystallizes in orthorhombic, space group Cmcm with a = 10.4210(6), b =23.3526(14), c = 6.9214(4) ?, V = 1684.37(17) ?3, Z = 4, C9H4N5O10Zn2, Mr = 472.91, Dc = 1.865g/cm3, F(000) = 932, λ(MoK α) = 2.909 mm-1, R = 0.0423 and wR = 0.1287. The complex has good thermal stability and excellent photoluminescent property.
  • DOI:

    10.14102/j.cnki.0254-5861.2011-1029

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    O641.4

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