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Syntheses and Crystal Structures of Two New Complexes Generated from 2-((Pyridin-3-ylmethyl)thio)-5-(6-quinolinyl)-1,3,4-oxadiazole and Ag~Ⅰ Salts

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【作者】 吴祥雯尹诗马建平

【Author】 WU Xiang-Wen;YIN Shi;MA Jian-Ping;College of Chemistry,Chemical Engineering and Materials Science,Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong,Key Laboratory of Molecular and Nano Probes,Ministry of Education,Shandong Provincial Key Laboratory of Clean Production of Fine Chemicals,Shandong Normal University;

【机构】 College of Chemistry,Chemical Engineering and Materials Science,Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong,Key Laboratory of Molecular and Nano Probes,Ministry of Education,Shandong Provincial Key Laboratory of Clean Production of Fine Chemicals,Shandong Normal University

【摘要】 Two new Ag-complexes have been synthesized based on the semi-rigid ligand 2-((pyridin-3-ylmethyl)thio)-5-(6-quinolinyl)-1,3,4-oxadiazole(L),obtained by the condensation reaction of 5-(6-quinolinyl)-1,3,4-oxadiazole-2-thiol and 3-chloromethyl pyridine hydrochloride. Crystallization of L with Ag OTf and Ag PF6 in a CH2Cl2/MeO H mixed solvent system at room temperature affords a novel supramolecular [Ag2L2(CF3SO32](I) and a coordination polymer [Ag L(PF6)]n(Ⅱ),respectively. Two complexes were characterized by TGA,X-ray powder and single-crystal diffraction.

【基金】 financially supported by the National Natural Science Foundation of China(No.21201112)
【所属期刊栏目】 organometallic structural chemistry (2016年12期)
  • 【DOI】10.14102/j.cnki.0254-5861.2011-1148
  • 【分类号】O641.4
  • 【被引频次】2
  • 【下载频次】14
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